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Advanced Materials

Alloying at high temperatures

In situ dendrite evolution in an aluminium-copper alloy captured using ultra-fast 3D tomography. Aluminium-rich dendrites are shown in (a, b, d, e). (c) and (f ) show smaller portions of the solid-liquid interface of (a) and (d) coloured according to the velocity of the moving surface with warmer colours, eg red and yellow, indicating faster growth of the dendrites.

Real-time imaging of the microstrucure of aluminium-copper alloys helps to optimize their mechanical properties.

Understanding the formation of materials at elevated temperatures is critical for determining their final properties. At the Swiss Light Source, a 300 W infrared laser heating system is available to provide controlled localised heating up to 1800º C.

In this example, as an aluminium-copper alloy was cooled from above the melting point, ultra-fast 3D x-ray tomographic microscopy captured the velocity of the evolving solid interface and dendrite growth with 1.1 µm pixel size. Real-time data on the solidification of the alloy revealed the formation of the microstructure and how fast the solid-liquid evolution occurred.

 

 

 

 

 

 

References

Development of a laser-based heating system for in situ synchrotron-based x-ray tomographic microscopy
Fife JL, Rappaz M, Pistone M, Celcer T, Mikuljan G, Stampanoni M
Journal of Synchrotron Radiation. 2012;19:352.
https://doi.org/10.1107/S0909049512003287

Financing of this work through the Swiss Competence Centre of Materials Science and Technology (CCMX) and its industry partners Asulab, Constellium, Kugler Bimetal, Novelis, Rolex and Varinor.